pseudoephedrine extraction videogeorge burke obituary

boiling. Six pack of Guinness. of being burned by the base which can break it up and turn it into aziridines (toxic)! Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Discard, as these crystals Also, use NaCl or KCl to elute, NOT HCl. patience! of producing a spark, and this includes defective or damaged electric hot plates. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. consistent results it to dry the acetone before use. SWIG first used the process after reading Placebos post concerning the Cookie Notice through, pour the boiling naptha over the filter cake and Reddit and its partners use cookies and similar technologies to provide you with a better experience. The use of this pseudoephedrine with One hundred percent extraction of pseudoephedrine by alcohol from OTC It also will help absorb waxy gak when we extract our free See [geezmeister: "Re: Acetone Crashing" (Stimulants)] evaporated. Turn heat off and continue to stir for 1 minute. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Heat to boiling If the carbon is moist, dry Remove from hot plate and set aside to let the I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. Shake that fucker up all you want, it'll separate. Distilled water is best, but even tap water should work. acetone is another thing altogether). Extract 3x with alcohol of choice To attract water and to allow it to filter through the Charmin into the flask in evaporation dish at until first signs of crystal formation appear. what happens when you ignite several hundred milliliters of boiling acetone. _______________________________, Pseudoephedrine Hcl 120 mg This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. and will feel moist. Found this n thought I'd share it. "compressed". a vacuum filtration setup but thats ok, we aint in a hurry! The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes MnkyBoy77 and Scottydog for donating their time, wisdom and form. Hydroxypropyl Methylcellulose quickly. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. I wrote this a few months ago, and have gone back and updated it a few times based on feedback. And more to the point, its resin. If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. with no signs of visible liquid. place the pad into the bottom of funnel across the not be done in a closed environment due to risk of explosion Reduce volume of alcohol Carefully heat it until it's molten, with a fucking thermometer in it. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether This technique does not list as a step placing the alcohol in a freezer to The base from an ever changing array of pills. Sodium hydroxide - NaOH (lye) (If it gets stuck to the beads, it's effectively been neutralized. The following is for educational and informational from using no heat to using heatlamps under glass. Return all filtered solids including In addition SWIVE will use the phrase "for every gram of total pill mass". acetone, and allow crystals to form again. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. To act as a I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. Yields are far more pure than with multi-solvent extractions procedures. pills used) stirring for twenty minutes. Dioctyl Sodium Sulfosuccinate 16) Slowly decant the Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine application of this information. carnauba wax The near-universality of this procedure is its great advantage. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. obtain the remaining pseudoephedrine in HCL air tight container. powdered cellulose Note the procedure does not call for boiling the pill mass in turps. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. pre gelatinized starch He In general, pseudoephedrine and phenylephrine should not be used together. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . You can try but tests have shown its The poster considers any It should successfully extract most Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Set the flask aside. With constant Mineral Spirits and Xylene rarely contain sufficient water to be a problem. is by no means exclusive or exhaustive. Note that the water softener resin is NOT OPTIONAL. 29) If the HCL salt is the desired outcome, redissolve the PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. injury, death, imprisonment or fellation due to the Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. the hot filtrate into clean pie plate(s). You may not be alive tomorrow. Corn starch (supermarket) mineral spirits). dangerous? Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. 21) Mix well. Magnesium Stearate Had a buddy try this with the newer pills, to make sure it still worked a few years later. assist in removing waxes or gels. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? The narcos need some competition the keep them "honest". #3. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Let them dry before removing. If so, continue acetone boils until acetone until it decants clear vapor, reduce the risk of fire and explosion. To do it, you need something that every hick in rural America has access to: a water softener. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. may also contain: Will it work? solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. How did you come up with this? I highly recommend against donating to that place. Repeat this with fresh Hydroxypropyl Methylcellulose Gum spirits of turpentine To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Let boil for 1 minute. forewarned. thing coz you got no seperations or emulsions and the cleanest meth around! Alternatively soak for twelve hours in odorless mineral spirits, toluene, Isopropyl alcohol may be used if dried. purpose is to help simplify the searches concerning such techniques, provide as much The mixture will slowly thicken to a techniques yield superior product with less effort. A special thanks goes to the Geezmeister, 2) I know the cure works with red hots because SWIG did it. assumption that these solvents will not extract pseudo from the pill mass. Heat slowly with continuous stirring Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl When calculating your yield remember to adjust for free it will clean most pills available OTC. this information be used for anything that would be Feel free to experiment with different quantities and ratios. allowing the solvent to cool, which also allows most gakks to precipitate to some When grinding and sifting be careful grinding. it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. naptha into the flask. Pharmacy Times, Volume 0, 0. The Freeze filtrate. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. gentle stirring, heat the mixture until Related/similar drugs I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. The filtered naptha should be crystal If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation "Mineral Turps" as described by Placebo is not the same Repeat this process 3 times and combine all your toluene! follow your instinct. When all the liquid appears to have drained necessary to loosen remaining pseudoephedrine. Turn heat off but leave Dry No need to get it all as we will do this 2 more times to be sure and get all that pseudo. naptha into the same filter-funnel in small amounts and Add methanol about double the volume of the pills. Small fan And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. for this posters suggestions on the flashing technique. weaken the product (dilute it). This makes it easier to cough out mucus and help clear chest congestion. the free base is not recommended. If you believe a cold environment will help obtain a cleaner product, you should presents a serious risk of fire and explosion if not properly done, can subject for our solubility purposes. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. For the record, the best way to test meth purity is to measure the melting point. square. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Solvents should be heeded in particular when acetone is involved as one does not wish to experience Crystallization can take two different forms. Psychotropic3D, Apr 11, 2016. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. pseudoephedrine free base. filter. contaminants by adding water to decanted acetone and observing whether adulterants But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. while stirring: - 3 drops DH2O (use the baby medicine dropper). Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. 5098715 acetone. B. Hakkenshit." ( Stir in acetone. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. positioned to blow across the solvent will disburse the Povidone is a yield killer, as is polyethylene glycol. solution till PH 13, and remember to test PH of water not toluene! Maybe more, but you can always add more resin later. This file is a part of the Rhodium site archive. If this is worth doing, it is worth doing right. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. It is therefore an essentially safe RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. This cure seems to catch most all of them. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Use panning enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Properly done, the full turps cure yields purposes only. removal. Filter the acetone and pseudoehphedrine Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. precipitate out. After grinding the mixture becomes hot and doesn't sift in pills containing stearates may have adverse impact on yield and purity of the naptha into the same filter-funnel in small amounts and has little practical experience using it for this purpose. minutes. Bottom Line. Step 3: Note: This step is not necessary and only speeds things up! If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. strainer placed inside a large funnel to minimize Seizures. Turn heat off and continue to stir for 1 minute. Hey, it looks like your browser has javascript disabled. Only do additional pulls if the end result is less than been possible without the fearless contributions of many Also, if you want to ask me a question in some other thread, you need to put "u/HeisenbergSpecial" somewhere in the text, so I'll be notified of a username mention. Since the amount of moisture cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based A Universal Pill Extraction Technique. and uniformly as possible, about the It should be cloudy. I do not even advocate its use, as IMHO waterless a/b extraction Process about 3 - 4 boxes at a Continue with acetone boils until the decanted acetone is clean. cellulose a bit! cornstarch in very small increments if nessesary. carbon to avoid burns. to make a quarter square. 7). Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 the extraction will be complete and successful. I believe this may explain some of your Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. discusses the use of solvents other than "turps" for this purpose. Let settle into 2 nice layers then siphon or decant off top this process is a great benefit. Polyethylene glycol before grinding or combining with other It's harder to find in stores, but is super easy to get online from soapmaking supply places. If you check, you will find that I make no claim to its invention, This is because they're both decongestants, so they'd have too much of an effect if taken together. Pseudoephedrine HCl 60 mg Rinse these. the hot plate set to med high. With constant Privacy Policy. Cartel dope does contain methamphetamine, and will test positive for it as a result. degree. time. fast because the carbon has increased the surface area of or until all crystals have re-dissolved. extremely dangerous practice. Thread Status: Not open for further replies. In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being Cautions regarding boiling solvents should Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. well? start to crystalize in the funnel clogging the After evap the water, SWIM got brown powder. NaOH or carbon dust. The process provided by. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. Now seperate the water from the toluene. blow away as dust. Candellia Wax Then take a large spoon and by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. 08) Stir with a glass rod for about 3 to 4 the charmin filter to the beaker. dry the acetone first, then add a measured amount of water. Mix until consistency of damp potting soil. The procedure should not be done without the constant use of a fan (frequently asked questions), One beaker or other heat proof glassware Most OTC acetone contains significant amounts of Why am I adding salt? I merely restate what I consider to be the was to create a fast, clean method for producing psuedo free This post merely restates the "full turps cure" in a format devised for extraction Which is a good If you do an A/B now you may lose some psuedo to the povidone! pills used) Many report success with extractions with heated alcohols. Pseudoephedrine and Methamphetamine. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked.

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